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Go To: Top IR Spectrum References Data from NIST Standard Reference Database 69: NIST Chemistry WebBook The National Institute of Standards and Technology (NIST) uses its best efforts to deliver a high quality copy of the Database and to verify that the data contained therein have been selected on the basis of sound scientific judgment

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We developed an alternative electrophilic aromatic substitution reaction for the organic chemistry teaching laboratory The experiment is an electrophilic iodination reaction of salicylamide a popular analgesic using environmentally friendly reagents—sodium iodide and bleach Further we designed the lab as a guided-inquiry experiment asking the students first to predict the

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Question: Below Is IR Spectrum After Iodination Of Salicylamide Was Performed A) Can Someone's Label All Peaks Special Between 700-900cm-1 And Determine Which Product Was Formed Out Of The List In The Page Below B) What Are The Possible Iodination Product C) Predict The Most Likely Site Of Iodination And Explain Your Reasoning? D) What Product Was Actually Produced?

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Figure 5 shows the IR spectrum of azintamide Clioquinol is synthesized by iodination of 5-chloro-8hydroxyquinoline hydrochloride by the following reaction (6): NoI + NaIO3 + H202 in C2HsOH OH OH The major impurity likely to be present in clioquinol active ingredient is the precursor 5-chloro-8-hydroxyquinoline Other potential impurities are 5 7-diiodo-8-hydroxyquinoline 5 7-dichloro

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Biocatalysis is an important adjunct to the chemical armamentarium that organic chemists may bring to bear for the synthesis of important intermediates and finished pharmaceutical and other commercial products For most of the world however such catalytic reagents are not an option due to their high cost and import limitations Recent studies indicate that the use of locally available

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Once the product was dried it was weighed and the

3 From the results gathered from the IR spectroscopy reading and melting points the end product was confirmed to be 5-Iodosalicylamide in a 1 2 4-trisubstituted ring The true melting point of this compound is 228C which is close to the melting point that was observed from the end product The percent yield was calculated to be ___% Questions 1 The IR spectrum of salicylamide is shown below

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The IR spectrum suggests meta substitution but if a group meta to the methyl substituent is present this group does not contain hydrogens since no other hydrogens are seen on the NMR spectrum The positive test for nitrogen however suggests that this group may be something like a nitrile group or a nitro group In the IR spectrum nitriles show a C==N stretch in the range of 2220-2260 cm

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